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- W2048967522 abstract "Poly(ethylene adipate), poly(ethylene suberate), and poly(ethylene sebacate) were synthesized by a modified ester interchange procedure. Polydispersity was reduced and low molecular weight material removed by fractional crystallization. Samples of 50–60% crystallinity were prepared by bulk crystallization and annealing. Melting points and amorphous densities were obtained by dilatometry. Melting points were 7–12°C higher than previously reported. Heats of fusion were measured by differential scanning calorimetry and extrapolated to 100% crystallinity by using measured amorphous densities and recently redetermined crystalline densities. Entropies of fusion were calculated and separated for the first time into volume expansion and conformational contributions." @default.
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- W2048967522 date "1970-08-01" @default.
- W2048967522 modified "2023-09-24" @default.
- W2048967522 title "Heats and entropies of fusion of linear aliphatic polyesters. I. Experimental determinations" @default.
- W2048967522 doi "https://doi.org/10.1002/pol.1970.160080810" @default.
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