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- W2048968314 abstract "Durch Tempern inniger Gemenge der Oxide RbO0,9 und Li[MnO4] (Rb:Mn = 1,5:1; Ag-Zylinder; 660°C, 56 d) wurden dunkelgrüne, orthorhombische Einkristalle von Rb2[MnO4] erhalten. Die Einkristallstrukturbestimmung belegt die Isotypie zu K2[MnO4]; es liegt der β-K2SO4-Typ vor. Somit konnten erstmals auf rein festkörperchemischem Weg, über einen reduktiven, vollständigen Alkalimetall-Austausch, Einkristalle eines Oxomanganates(VI) der Alkalimetalle dargestellt werden. Der Madelung-Anteil der Gitterenergie, MAPLE, sowie die Ladungsverteilung wurden berechnet. A ‘Reductive Exchange Reaction’: Single Crystals of Rb2[MnO4] from Li[MnO4] By heating of well ground mixtures of the oxides RbO0.9 and Li[MnO4] (Rb:Mn = 1.5:1; Ag-tubes; 660°C, 56 d) dark-green, orthorhombic single-crystals of Rb2[MnO4] were obtained. The structural determination revealed the isotype to K2[MnO4]; a β-K2SO4-typ. Thus, for the first time by a pure solid-state-chemical way, via a reductive, complete alkali-metal exchange, single crystals of an oxomanganate(VI) of the alkali metals were prepared. The Madelung Part of the Lattice Energy, MAPLE, and the charge distribution were calculated." @default.
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- W2048968314 date "1995-02-01" @default.
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- W2048968314 title "Eine ?Reduktive Austausch-Reaktion?: Einkristalle von Rb2[MnO4] aus Li[MnO4]" @default.
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- W2048968314 doi "https://doi.org/10.1002/zaac.19956210202" @default.
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