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- W2049093635 abstract "We report the first synthesis of the unnatural enantiomer of desmosterol (ent-desmosterol). The sterol nucleus was constructed enantiospecifically, followed by stepwise addition of the side chain. Beginning with ent-androst-4-ene-3,17-dione, ent-desmosterol was synthesized in 13 steps and 20% yield. Protected ent-desmosterol was subjected to catalytic deuteration to afford ent-deuterocholesterol. Ent-desmosterol and ent-deuterocholesterol will be used to study the importance of sterol absolute configuration for sterol-lipid interactions in biophysical studies and in biological systems." @default.
- W2049093635 created "2016-06-24" @default.
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- W2049093635 date "2003-02-01" @default.
- W2049093635 modified "2023-09-23" @default.
- W2049093635 title "First synthesis of ent-desmosterol and its conversion to ent-deuterocholesterol" @default.
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- W2049093635 doi "https://doi.org/10.1016/s0039-128x(02)00174-5" @default.
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