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• W2049102504 abstract "The reactions (I) Hg2Cl2(s) + Br2(g) and (II) HgCl2(s) + HgBr2(s) have been investigated by an X-ray method. Both the reactions yield two forms of the mixed halide HgClBr, designated as α-HgClBr and β-HgClBr. The cell parameters of the two are as follows: α-HgClBr: a = 6.196 Å, b = 13.12 Å, c = 4.37 Å, z = 4, ϱ = 5.91 g/cm3. The powder pattern and cell parameters are similar to that of HgCl2. Therefore it is probable that the chlorine atoms, in the linear halogenHghalogen molecules of HgCl2 structure have been replaced by bromines, and since the radius of the bromine atom is larger than that of chlorine, the lattice is larger in this case. β-HgClBr: a = 6.78 Å, b = 13.175 Å, c = 4.17 Å, z = 4, ϱ = 5.40. These parameters are the same as those reported in the literature for β-Hg(ClBr)2, and its X-ray powder pattern is similar to HgCl2. Therefore this phase also has linear halogenHghalogen molecules but the distribution of Cl and Br atoms is perhaps random. Heating the products (I) and (II) up to the melting point increases the amount of α phase and decreases the β phase, whereas crystallization increases the β phase. DTA study has supported the X-ray findings." @default.
• W2049102504 created "2016-06-24" @default.
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• W2049102504 date "1981-11-01" @default.
• W2049102504 modified "2023-10-18" @default.
• W2049102504 title "X-ray study of Hg2Cl2Br2 and HgCl2HgBr2 reactions in solid state" @default.
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• W2049102504 doi "https://doi.org/10.1016/0022-4596(81)90370-4" @default.
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