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- W2049120161 abstract "Abstract Five complexes of the bromides of La, Nd, Gd, Ho and Er with 4-N-(2′-hydroxy-1′-naphthylidene)aminoantipyrine (HNAAP) of the general composition [Ln(HNAAP)2Br2]Br where Ln=La, Nd, Gd, Ho and Er have been synthesised and characterised. Electronic and infrared spectra of the complexes indicate the weak covalent character of the metal-ligand bond and the neutral tridentate behaviour of the ligand. Thermogravimetric studies of the complexes in nitrogen atmosphere indicate that these complexes are stable upto about 240°C and undergo decomposition in two stages forming the respective metal bromides as the final products. The lunetic parameters for the first decomposition stage were calculated using the Coats-Redfern equation. The rate controlling process for the first stage obeys the Ginstling-Brounshtein model which represents three-dimensional diffusion with spherical symmetry. There is no regular variation in the values of the kinetic parameters of the decomposition of the complexes as with other common physical constants." @default.
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- W2049120161 date "1998-03-01" @default.
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- W2049120161 title "Synthesis, Spectral and Thermal Studies on Bromide Complexes of La(III), Nd(III), Gd(III), Ho(III) And Er(III) with 4-N-(2′-Hydroxy-1′-Naphthylidene)Aminoantipyrine" @default.
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- W2049120161 doi "https://doi.org/10.1080/00945719809349359" @default.
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