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- W2049179623 abstract "Durch Lithiierung von silylierten Aminen und Anschließende Umsetzung mit Imidhalogeniden werden, ebenso wie im Falle der Reaktion von N,N′-Diphenylfromylamidin mit Chlortrimethylsilan und Triäthylamin, Silylamidine erhalten. Setzt man N,N′-Dimethyl-N-trimethylsilyl-äthylendiamin mit n-Butyl-lithium und Imidhalogeniden um, so erhält man Trimethylsilylaminoalkylamidine. Bei der Reaktion der Silylamidine bzw. der Trimethylsilylaminoalkyl-amidine mit Halogendiorganylboranen erhält man die entsprechenden Amidinoborane. Die verbindungen werden analytisch und spektroskopisch (1H-, 11B-, 19FNMR; MS; IR) charakterisiert. Reaction of Metal and Metalloid Compounds with Polyfunctional Molecules. XVII. Synthesis of Silylamidines and their Reaction with Boranes By silylation of lithiated amines and subsequent reaction with imid halides, as well as by reaction of N,N′ -diphenylformylamidine with chlorotrimethylsilane and triethylamine, silylamidines were obtained. By reaction of N,N′-dimethyl-N-trimethylsilylethylenediamine with n-butyl-lithium and imid halides, trimethylsilylaminoalkylamidines are formed. By reacting silylamidines or trimethylsilylaminoalkylamidines with halogenodiorganylboranes the corresponding amidinoboranes were synthesized. 1H, 11B, 19F n.m.r. spectra, mass spectra and characteristic i.r. group frequencies are reported." @default.
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- W2049179623 date "1978-10-01" @default.
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- W2049179623 title "Umsetzungen von metall- und Metalloidverbindungen mit mehrfunktionellen Molek�len. XVII. Synthese von Silylamidinen und deren Umsetzung mit Boranderivaten" @default.
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- W2049179623 doi "https://doi.org/10.1002/zaac.19784450114" @default.
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