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- W2049202370 abstract "Für eine neue Insulin-Synthese wird unter Umgehung des Schwefelschutzgruppen-Problems das geschützte Bis-hexadecapeptid (B 1-16)2, [Z-Phe-Val-Asn-Gln-His-Leu-Cys(−)-Gly-Ser(But)-His-Leu-Val-Glu(OBut)-Ala-Leu-Tyr(But)-OMe]2 (15), durch Azidkupplung des Disulfids der Sequenz (B 1-8)2 (8) mit überschüssigem Octapeptid-Derivat B 9-16 (13) hergestellt. 8 wird durch stufenweise Kettenverlängerung unter Verwendung von [Z-Cys(−)-ONp]2 erhalten. Peptides, LXXIV1). Synthesis of the Insulin Sequence (B 1-16)2 as a Symmetrical Disulfide2) In order to synthesize insulin by a method avoiding the problems of sulfur protecting groups, the protected bishexadecapeptide (B 1-16)2, [Z-Phe-Val-Asn-Gln-His-Leu-Cys(−)-Gly-Ser(But)-His-Leu-Val-Glu-(OBut)-Ala-Leu-Tyr(But)-OMe]2 (15), is synthesized by an azide coupling of the disulfide (B 1-8)2 (8) with an excess of the octapeptide derivative B 9-16 (13). 8 is obtained by a stepwise procedure using [Z-Cys(−)-ONp]2." @default.
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- W2049202370 date "1970-02-11" @default.
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- W2049202370 title "Peptide, LXXIV1) Synthese der Insulin-Sequenz (B 1-16)2 als symmetrisches Disulfid2)" @default.
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- W2049202370 doi "https://doi.org/10.1002/jlac.19707310112" @default.
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