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- W2049208243 abstract "X-ray evanescent wave-induced fluorescence (XEWIF) has been used to measure the monomer segment profile of poly(dimethylsiloxane) adsorbed from a dilute solution in bromocyclohexane to the solution/vapour interface. Rather than employment of a fluorescent label on the polymer chain, the bromine in the solvent provided the fluorescent label and sufficient intensity was observed to perform the experiments using a conventional X-ray source. The theta-point for this system has been reported as 29 °C and our measurements were performed at (23 ÷ 24) °C with no indication of bulk phase separation. Our results cannot be interpreted by scaling or mean-field models for polymer adsorption from a theta solvent. However, a step profile, in which a polymer-rich phase with polymer = 0.32 ± 0.02 extends (14 ± 3) nm into the bulk phase fits the data well. The step profile is consistent with the interpretation of prewetting near the solution critical point." @default.
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- W2049208243 date "1992-02-01" @default.
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- W2049208243 title "X-Ray Evanescent Wave-Induced Fluorescence Study of Polymer Adsorption below the Theta-Point" @default.
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- W2049208243 doi "https://doi.org/10.1209/0295-5075/17/5/004" @default.
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