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- W2049209614 startingPage "2503" @default.
- W2049209614 abstract "The complexes [Fel2(CNR)4](R = Ph, p-MeC6H4 or But) react with Hg in the presence of CNR to give [(RNC)5Fe → HgI2], and exchange reactions with AgX (X = Br or Cl) lead to the corresponding halogeno-complexes [(RNC)5Fe → HgX2]. Treatment with 1 mol of AgClO4 affords the cationic complexes [(RNC)5Fe–HgX]ClO4 which are unstable towards mercury extrusion. The relative stability of the complexes is discussed in terms of the influence of the ligands co-ordinated to Hg and the steric and electronic characteristics of the RNC ligands. The structure of [(p-MeC6H4NC)5Fe → HgI2] has been determined: monoclinic, space group P21/a, a= 16.680(3), b= 18.031(4), c= 15.256(2)Å, β= 116.92(2)° and Z= 4." @default.
- W2049209614 created "2016-06-24" @default.
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- W2049209614 date "1991-01-01" @default.
- W2049209614 modified "2023-10-16" @default.
- W2049209614 title "Insertion of mercury into iron–halogen bonds. X-Ray structure of [(p-MeC<sub>6</sub>H<sub>4</sub>NC)<sub>5</sub>Fe → HgI<sub>2</sub>]" @default.
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- W2049209614 doi "https://doi.org/10.1039/dt9910002503" @default.
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