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- W2049215512 abstract "The effect of temperature on the spin–lattice (R1) and spin–spin (R2) 13C relaxation rates of gluconate and manganese (II)–gluconate interactions was determined in D2O. An R2 vs T−1 minimum was observed for gluconate similar to that observed in solid-liquid phase transitions. Nuclear Overhauser enhancement factors indicated predominately dipolar relaxation mechanisms for all atoms except the carbonyl carbon. Activation energies and chemical shifts indicated a molecular reorientation involving the carbonyl carbon which resulted in changes in solvation effects. Addition of manganese(II) to gluconate in D2O resulted in an observed minimum in the R1 vs T−1 plots for all carbon atoms except the carbonyl species. The activation energies further supported the concept of changes in solvent-manganese-gluconate interactions produced by variations in intramolecular structure." @default.
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- W2049215512 title "Carbon-13 NMR relaxation studies of gluconate and manganese—gluconate interactions" @default.
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- W2049215512 doi "https://doi.org/10.1002/mrc.1260260711" @default.
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