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- W2049279030 abstract "Abstract To ascertain the effect of a replaceable hydrogen on deuterium incorporation, 2‐pentynol, 2‐hexynol, 3‐hexynol, their tetrahydropyranyl (THP) ethers, and the mono‐ and di‐THP ethers of 3‐hexyne‐1,6‐diol were deuterated catalytically with deuterium gas. The differences in percent d 4 (using Wilkinson's catalyst, tris (triphenylphosphine)‐chlororhodium) or percent d 2 (using Lindlar's catalyst, Pd on CaCO 3 poisoned with a lead salt) measured for the alcohols and their THP ethers were, in general, less than 4% with either catalyst. Noticeable exceptions occurred during the deuteration over Wilkinson's catalyst of 2‐pentynol and 2‐hexynol; extensive scatter resulted in a substantial decrease in percent d 4 . This scatter was not observed with the corresponding THP ethers." @default.
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- W2049279030 date "1992-07-01" @default.
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- W2049279030 title "Catalytic deuteration of alkynols and their tetrahydropyranyl ethers" @default.
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- W2049279030 doi "https://doi.org/10.1007/bf02536142" @default.
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