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• W2049291247 abstract "Dispersive X-ray absorption fine structure (XAFS) spectroscopy was used to monitor changes in the Pt charge and the number of O and Pt nearest neighbors during the electrochemical oxidation and reduction of a dispersed Pt catalyst in real time. The oxidation at 1.20 V/SHE follows logarithmic kinetics over a period of 5 min with all three XAFS features (NO, NPt and the absorption peak) changing identically. However, the reduction at 0.10 V is well fitted by a single exponential on a similar time-scale with NPt changing at half the rate at which NO and absorption peak are changing. When combined with the direct quantitative structural information obtained from XAFS, we find that these reactions on clusters apparently proceed by a different mechanism from that on bulk platinum electrodes in aqueous solution and also suggest a mechanism for the platinum restructuring during these reactions. Therefore the behavior of the clusters may differ from that of bulk electrode surfaces." @default.
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• W2049291247 date "1995-03-01" @default.
• W2049291247 modified "2023-09-24" @default.
• W2049291247 title "Direct observation of surface oxide formation and reduction on platinum clusters by time-resolved X-ray absorption spectroscopy" @default.
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• W2049291247 doi "https://doi.org/10.1016/0022-0728(94)03635-g" @default.
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