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• W2049654881 abstract "Standard values of Gibbs free energy, entropy, and enthalpy of Na2Ti6O13 and Na2Ti3O7 were determined by evaluating emf-measurements of thermodynamically defined solid state electrochemical cells based on a Na–β″-alumina electrolyte. The central part of the anodic half cell consisted of Na2CO3, while two appropriate coexisting phases of the ternary system Na–Ti–O are used as cathodic materials. The cell was placed in an atmosphere containing CO2 and O2. By combining the results of emf-measurements in the temperature range of 573⩽T/K⩽1023 and of adiabatic calorimetric measurements of the heat capacities in the low-temperature region 15⩽T/K⩽300, the thermodynamic data were determined for a wide temperature range of 15⩽T/K⩽1100. The standard molar enthalpy of formation and standard molar entropy at T=298.15 K as determined by emf-measurements are ΔfHm0=(−6277.9±6.5) kJ · mol−1 and Sm0=(404.6±5.3) J · mol−1 · K−1 for Na2Ti6O13 and ΔfHm0=(−3459.2±3.8) kJ · mol−1 and Sm0=(227.8±3.7) J · mol−1 · K−1 for Na2Ti3O7. The standard molar entropy at T=298.15 K obtained from low-temperature calorimetry is Sm0=399.7 J · mol−1 · K−1 and Sm0=229.4 J · mol−1 · K−1 for Na2Ti6O13 and Na2Ti3O7, respectively. The phase widths with respect to Na2O content were studied by using a Na2O-titration technique." @default.
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• W2049654881 date "2003-09-01" @default.
• W2049654881 modified "2023-10-16" @default.
• W2049654881 title "Thermodynamic properties of Na2Ti6O13 and Na2Ti3O7: electrochemical and calorimetric determination" @default.
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• W2049654881 doi "https://doi.org/10.1016/s0021-9614(03)00125-3" @default.
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