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- W2049693585 abstract "A vibrating capacitor device (Kelvin probe) has been developed for measurements of work-function changes ΔΦ during ongoing catalytic reactions up to high temperatures (750 K) and atmospheric pressure. The construction is based on the piezoelectric actuator principle, and utilizes a lever arrangement that transfers the vibrating motion of the actuator to the reference electrode. The lever arrangement eliminates a static load on the actuator, which therefore allows a large distance between the actuator and the vibrating reference electrode. This makes possible much higher temperatures in the reaction/sample zone than the piezoelectric actuator itself permits. The large actuator–electrode distance also reduces the risk of electromagnetic pickup in the ΔΦ measurements, from the driving circuit for the piezoelectric actuator. The reference electrode is a gold disk with 3 mm diameter and a thickness of 0.1 mm. The practical ΔΦ resolution is presently about 5 meV. The device has been combined with on-line mass spectrometric detection of reaction rates and its performance is illustrated by results from the H2/O2 and CO/O2 reactions on Pt." @default.
- W2049693585 created "2016-06-24" @default.
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- W2049693585 date "1995-07-01" @default.
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- W2049693585 title "A high‐temperature Kelvin probe for flow reactor studies" @default.
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- W2049693585 doi "https://doi.org/10.1063/1.1145403" @default.
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