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- W2049759787 abstract "The asymmetric synthesis of the cyclohexyl fragment of FK-506 is reported. This new synthesis (five steps, 30% overall yield) starts, for the first time, from (S)-(−)-3-cyclohexenecarboxylic acid (S-2) instead of the commonly used R form (acid R-2) and utilizes an epimerization reaction. The overall yield is improved to 35% by recycling recovered starting product (hydroxy ester 7c) from the epimerization step." @default.
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- W2049759787 date "1992-01-01" @default.
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- W2049759787 title "Practical, asymmetric synthesis of the cyclohexyl C28-C34 fragment of the immunosuppressant FK-506 via (S)-(−)-3-cyclohexenecarboxylic acid" @default.
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- W2049759787 doi "https://doi.org/10.1016/s0040-4020(01)89015-3" @default.
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