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• W2049833384 abstract "Partially deuteriated 1,5,6,6-(2)H(4)-d-glucose and 1(I),1(II),5(I),5(II),6(I),6(I),6(II),6(II)-(2)H(8)-d-cellobiose were synthesized in high yields and on a large scale from d-glucose. (2)H enrichment at C-5 and C-6 of each glucopyranosyl unit in excess of 85% and 90%, respectively, was realized by (1)H-(2)H exchange in (2)H(2)O containing deuteriated Raney Ni. Nucleophilic addition of LiAlD(4) to 5,6,6-(2)H(3)-2,3,4,6-tetra-O-benzyl-d-gluconolactone led to a 98% (2)H enrichment at C-1. Deuteriated cellobiose is of interest as building block for the synthesis of a model compound of cellulose I." @default.
• W2049833384 created "2016-06-24" @default.
• W2049833384 creator A5055827041 @default.
• W2049833384 creator A5075695962 @default.
• W2049833384 date "2007-12-01" @default.
• W2049833384 modified "2023-10-11" @default.
• W2049833384 title "Regioselective synthesis of 1I,1II,5I,5II,6I,6I,6II,6II-2H8-cellobiose" @default.
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• W2049833384 doi "https://doi.org/10.1016/j.carres.2007.07.017" @default.
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