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- W2050443389 abstract "The title compounds 3 and 7 are novel heterocyclic systems incorporating two-coordinate phosphorus. They are obtained in reasonable to good yields from the condensation of suitable 2-ethyl-3-alkylthiazolinium and -benzothiazolium bromides 2 and 6 with phosphorus trichloride in the presence of triethylamine in an aprotic solvent. Intermediate dichlorophosphino-substituted N-ylides can be observed or isolated in some cases. From a 2-methyl-3-alkylthiazolinium bromide (2a), a 1-(dichlorophosphino) substituted 1, 3-azaphospholo[5,1-b]thiazoline (4) was obtained. The chemical shift of the two-coordinate phosphorus in 1,3-azaphosphole derivatives clearly reflects the influence of the heterocyclic system annulated to its 1,5-bond and of the substituents in its 2-and 4-positions." @default.
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- W2050443389 date "1992-08-01" @default.
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- W2050443389 title "1, 3-azaphospholo[5, 1-b]thiazolines and benzothiazoles" @default.
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- W2050443389 doi "https://doi.org/10.1002/hc.520030408" @default.
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