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- W2050794310 abstract "The transformation of the end groups of polyethylene glycol to the O-ethoxycarbonylmethyl derivative 2 is described, using either a base-catalysed reaction with ethyl bromoacetate or an acid-catalysed reaction with ethyl diazoacetate. Compound 2 was reacted with methyllithium or methylmagnesium iodide to yield the α, ω title compounds. The end hydroxyl grouping of polyethylene glycol monomethyl ether was similarly transformed. Yields, experimental convenience and eventual side reactions are discussed." @default.
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- W2050794310 date "2010-09-01" @default.
- W2050794310 modified "2023-09-23" @default.
- W2050794310 title "Synthesis of α-(2-Hydroxy-2, 2-Dimethylethyl)-ω-Methyl-, and of α ω-Bis (2-Hydroxy-2,2-Dimethylethyl) Polyethylene Glycol" @default.
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- W2050794310 doi "https://doi.org/10.1002/bscb.19860950407" @default.
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