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- W2050813817 abstract "Mit Hilfe von Schmelzflußreaktionen wurden Einkristalle der bisher unbekannten Verbindungen Ni5VB2O10 (I) und Ni5MnB2O10(11) erhalten. Beide sind isotyp zu Ni5TiB2O10, (Raumgruppe D2h9–Pbam, Z = 2; (I): a = 9,183; b = 12,189; c = 2,989 Å; (II): a = 9,130; b = 12,164; c = 2,970 Å). Ni2+ und V4+ bzw. Mn4+ besetzen eine der Metallpunktlagen statistisch. Die partielle Unordnung in der Metallverteilung wird durch Berechnung des Coulombterms der Gitterenergie bestätigt. About the Stabilization of the Oxidation State MIV in the Ni5MB2O10-Type (MV4+, Mn4+) The so far unknown compounds Ni5VB2Ol0(I) and Ni5MnB2O10(II) were prepared for the first time by using a flux growth. The obtained single crystals are isotypic to Ni5TiB2O10 (space group D–Pbam, Z = 2, (I): a = 9.183; b = 12.189; c = 2.989 Å (II): a = 9.130; b = 12.164; c = 2.970Å). One of the metal points positions is occupied statistically by Ni2+ and V4+ or Mn4+, respectively. The partial disorder in respect to the metal distribution is confirmed by calculations of the coulomb term of the lattice energy." @default.
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- W2050813817 date "1989-01-01" @default.
- W2050813817 modified "2023-09-25" @default.
- W2050813817 title "Zur Stabilisierung der Oxidationsstufe MIV im Ni5MB2O10-Typ" @default.
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- W2050813817 doi "https://doi.org/10.1002/zaac.19895790112" @default.
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