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• W2050871497 abstract "Für NMR-Diffusionsmessungen wurde ein z-Gradientensystem zur Erzeugung intensiver Feldgradientenimpulse überarbeitet. Dazu wurde das Gradientenfeld einer aktiv abgeschirmten Spule mittels der Finite-Elemente-Methode optimiert. Das System wurde aus Glaskeramik als Spulenträger aufgebaut. Es besitzt kein 1H-NMR-Eigensignal und weist einen hohen Strom/Gradienten-Wandlerfaktor von 0,37 T m–1A–1 auf. Mit dem Nachweis isotroper und anisotroper Diffusion in wässrigen Lösungen eines PEO-PPO-PEO Triblock-Copolymers und adsorbierten Methans in zwei verschiedenen mikroporösen kristallinen Adsorbentien wird die Funktionstüchtigkeit des Systems demonstriert. A z-gradient system for NMR diffusion measurements with intensive pulsed field gradients was redesigned. The gradient field of an actively screened gradient coil was optimized using finite element analysis. The gradient system was constructed with glass ceramic as coil support material. It does not show any background 1H NMR signal and has a high current-to-gradient conversion factor of 0.37 T m–1A–1. The functionality of the system for studying slow diffusion processes in interface systems is demonstrated by observing isotropic and anisotropic diffusion in aqueous solutions of a PEO-PPO-PEO triblock copolymer and of methane in two different microporous crystalline absorbencies." @default.
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• W2050871497 date "2013-09-18" @default.
• W2050871497 modified "2023-10-16" @default.
• W2050871497 title "Konstruktion und Test eines Gradientensystems für NMR-Diffusionsuntersuchungen in Grenzflächensystemen" @default.
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• W2050871497 doi "https://doi.org/10.1002/cite.201300087" @default.
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