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- W2051036613 abstract "Determination of TiOCl 2 in refined TiCl 4 was significant for analysis of its impurities. TiOCl 2 could be determined by infrared spectroscopy due to its infrared characteristic spectrum line. However, normal infrared absorption cell was not fit for the sample analysis, because TiCl 4 easily reacted with moisture in the air and immediately was hydrolyzed to form highly corrosive hydrochloric acid smoke. The infrared absorption cell with the window film of ZnSe ( Ф10×1mm, wavenumbers: 7800cm -1 ~440cm -1 ) and the glass cell (optical path: 22mm, 12mm, 7mm and 4mm) was assembled and utilized in determination of the TiOCl 2 in refined TiCl 4 by standard addition method. The detection limit of TiOCl 2 was 26.5mg•kg -1 , the regression equation was Y=1.0118X, R 2 =0.9926; With standard addition method, the regression equation of TiOCl 2 was Y=1.9400X, R 2 =0.9940,This infrared absorption device was safe, simple and convenient, easily removable and washable, and re-useable. This method could meet the requirement of determination of TiOCl 2 in refined TiCl 4 ." @default.
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- W2051036613 date "2014-08-01" @default.
- W2051036613 modified "2023-09-27" @default.
- W2051036613 title "Determination of Titanium Oxychloride in Refined Titanium Tetrachloride by Infrared Spectroscopy" @default.
- W2051036613 cites W2007216140 @default.
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- W2051036613 doi "https://doi.org/10.4028/www.scientific.net/amr.997.475" @default.
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