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• W2051205879 abstract "Abstract In this research, in situ fabrication of Al 3 V based nanocomposite and its formation mechanism have been investigated. In order to synthesize Al 3 V/Al 2 O 3 nanocomposite, a mixture of Al and V 2 O 5 powders was subjected to high-energy ball milling and the nanocomposite was produced through a mechanochemical reaction. The produced structure was isothermally heat-treated at 500–600 °C for 0.5–2 h under argon atmosphere. In order to evaluate the structural changes during milling and annealing, the synthesized powders were characterized by X-ray diffraction (XRD). Moreover, the powder morphological changes were studied by scanning electron microscopy (SEM). It was observed that the reaction between Al and V 2 O 5 occurred after about 30 min and, the Al 3 V and Al 2 O 3 were formed in nanocrystalline structure with the continuing mechanical milling. Calculation of adiabatic temperature confirmed that reaction took place in combustion mode. In final stage of milling up to 40 h; it was observed that the Al 3 V decomposed to Al and V so that the optimum time of milling to achieve fabrication of nanocomposite was determined to be about 20 h. Calculations based on Miedema’s model verified partial disordering of Al 3 V during further milling and annealing of as-milled powder at 600 °C led to the ordering of Al 3 V. The crystallite size of Al 3 V and Al 2 O 3 after annealing at 600 °C for 2 h remained in nanometer scale. So the final product appeared to be stable even after annealing." @default.
• W2051205879 created "2016-06-24" @default.
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• W2051205879 date "2013-01-01" @default.
• W2051205879 modified "2023-09-27" @default.
• W2051205879 title "In-situ fabrication of Al3V/Al2O3 nanocomposite through mechanochemical synthesis and evaluation of its mechanism" @default.
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• W2051205879 doi "https://doi.org/10.1016/j.apt.2012.03.004" @default.
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