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• W2051205937 abstract "A novel rhenium(IV)–rhenium(V) compound of formula NBu4[ReVO2(py)4][ReIVBr6] (1) (NBu4+ = tetra-n-butylammonium cation and py = pyridine) has been prepared and characterized. The crystal structure of 1 was determined by single crystal X-ray diffraction. 1 crystallizes in the monoclinic system with space group Cc. The rhenium(IV) ion is six-coordinate by six Br atoms [average value of the ReIV–Br bonds lengths being ca. 2.509(1) Å], while rhenium(V) ion is six-coordinate by two axial oxo groups and four N atoms from four pyridine ligands [average values of the ReVO and ReV–N bonds lengths being ca. 1.77 and ca. 2.14 Å, respectively]. The magnetic properties were investigated from susceptibility measurements performed on a polycrystalline sample of 1. Its magnetic behavior is that of a magnetically diluted Re(IV) complex and is interpreted in terms of magnetically isolated spin quartets with a high value of the zero-field splitting (|2D| is ca. 8.6 cm−1)." @default.
• W2051205937 created "2016-06-24" @default.
• W2051205937 creator A5022412014 @default.
• W2051205937 date "2014-01-01" @default.
• W2051205937 modified "2023-10-14" @default.
• W2051205937 title "Hexabromorhenate(IV) salt of a trans-dioxorhenium(V) cation: X-ray structure and magnetic properties" @default.
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• W2051205937 doi "https://doi.org/10.1016/j.poly.2013.09.003" @default.
• W2051205937 hasPublicationYear "2014" @default.
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