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- W2051212727 abstract "A novel pathway to enantiomerically pure 2,2′-dihydroxymethyl-1,1′-binaphthyl is described, through kinetic resolution of its racemic 7-membered biaryl lactone precursor. Oxazaborolidine-assisted borane reduction of this lactone proceeds with very high enantioselectivity (krel=50). For optimum results on a preparative scale, a ‘three fractions strategy’ is suggested, which combines kinetic resolution and fractional crystallization and leads to both atropisomers in high enantiomeric excess." @default.
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- W2051212727 date "1997-12-01" @default.
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- W2051212727 title "Efficient kinetic resolution of a racemic 7-membered biaryl lactone: enantioselective synthesis of 2,2′-dihydroxymethyl-1,1′-binaphthyl" @default.
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- W2051212727 doi "https://doi.org/10.1016/s0957-4166(97)00602-2" @default.
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