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• W2051218639 startingPage "914" @default.
• W2051218639 abstract "The synthesis of nanocrystalline solid solutions of general formula CexZr1−xO2 (x = 0.1, 0.25, 0.5, 0.75, and 0.9) using a citrate complexation technique was followed with thermochemical methods, and the resulting powders were characterized using X-ray diffraction (XRD) and electron microscopy (scanning electron microscopy and high-resolution transmission electron microscopy (HRTEM)). Qualitative analysis of XRD data indicated that the samples exhibited either a cubic (Fm3m) or a tetragonal (P42/nmc) phase, depending on CeO2 content. Electron diffraction results were consistent with the XRD findings. In HRTEM, the internal crystal structure of the nanoparticles was observed to be highly ordered and primary particle size data were collected. Average crystallite size, obtained from the XRD data, was 4.8−8.3 nm, with the larger values at the compositional extremes. A similar trend was observed in HRTEM, although values were generally slightly higher. The Ce0.5Zr0.5O2 solid solution had the smallest crystallites (4.8 nm) and the highest specific surface area (45.8 m2·g−1)." @default.
• W2051218639 created "2016-06-24" @default.
• W2051218639 creator A5044765163 @default.
• W2051218639 creator A5077444814 @default.
• W2051218639 date "2008-12-30" @default.
• W2051218639 modified "2023-10-17" @default.
• W2051218639 title "Synthesis of Nanocrystalline CeO₂−ZrO₂ Solid Solutions by a Citrate Complexation Route: A Thermochemical and Structural Study" @default.
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• W2051218639 doi "https://doi.org/10.1021/jp808825c" @default.
• W2051218639 hasPublicationYear "2008" @default.
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