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• W2051219751 abstract "The oxidation of benzylpyridines forming benzoylpyridines was achieved based on a synergistic H4NI–AcOH catalyst and molecular oxygen in high yield under solvent-free conditions. This is the first nonmetallic catalytic system for this oxidation transformation using molecular oxygen as the oxidant. The catalytic system has a wide scope of substrates and excellent chemoselectivity, and this procedure can also be scaled up. The study of a preliminary reaction mechanism demonstrated that the oxidation of the Csp3–H bonds of benzylpyridines was promoted by the pyridinium salts formed by AcOH and benzylpyridines. The synergistic effect of H4NI–AcOH was also demonstrated by control experiments." @default.
• W2051219751 created "2016-06-24" @default.
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• W2051219751 date "2015-04-17" @default.
• W2051219751 modified "2023-09-23" @default.
• W2051219751 title "Synergistic H₄NI–AcOH Catalyzed Oxidation of the C_sp³–H Bonds of Benzylpyridines with Molecular Oxygen" @default.
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• W2051219751 doi "https://doi.org/10.1021/acs.orglett.5b00602" @default.
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