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- W2051228550 abstract "In the reaction of (3,5-dimethyl-1H-pyrazol-1-yl)methyldiphenylphosphinite (dmpmp) with [PdCl2(CH3CN)2], we have obtained hydrolysis and phosphorus oxidation products and the unexpected complex cis-[PdCl2(dmbpm)] (dmbpm = bis(3,5-dimethyl-1H-pyrazol-1-yl)methane). Modifications in the synthesis of dmpmp (high temperature, strong base, and the presence of Ph2P(O)Cl) show that dmbpm is a by-product from the synthetic route to dmpmp. The complex cis-[PdCl2(dmbpm)] is isolated and fully characterized by mass spectrometry, analytical, and spectroscopy techniques and the crystal structure is obtained by X-ray diffraction methods." @default.
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- W2051228550 date "2009-12-20" @default.
- W2051228550 modified "2023-10-18" @default.
- W2051228550 title "Cleavage of NpzCH2 -OP and unexpected formation of bis(3,5-dimethyl-1H-pyrazol-1-yl)methane (dmbpm): X-ray crystal structure of [PdCl2(dmbpm)]" @default.
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- W2051228550 doi "https://doi.org/10.1080/00958970903208292" @default.
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