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- W2051230513 abstract "Palladium(0)-catalyzed alkylation of 2,3-unsaturated aryl glycoside with ethyl nitroacetate or N-(diphenylmethylene)glycine ethyl ester in the presence of N,O-bis(trimethylsilyl)acetamide/KOAc afforded ethyl 2-(4,5-di-O-benzyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2(R,S)-nitroacetate (2) and ethyl 2-(4,6-di-O-benzyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2(R,S)-[(N-diphenylmethylene)amino)]acetate (7), respectively. Hydrogenation of compound 2 afforded the saturated aminoesters, while compound 7 was readily transformed into 2-(4,6-di-O-benzyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2(R,S)-glycine (10) by acidic hydrolysis followedby saponification." @default.
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- W2051230513 date "2001-03-31" @default.
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- W2051230513 title "SYNTHESIS OF UNSATURATEDC-GLYCOSYL GLYCINES" @default.
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- W2051230513 doi "https://doi.org/10.1081/car-100103957" @default.
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