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- W2051236656 abstract "Abstract A recycled-flow NMR system is evaluated for application to two-dimensional 13C-1H J-resolved experiments. For proper choice of measurement conditions, it is demonstrated that spectral sensitivity enhancement is inversely proportional to 1 − exp ( −t a T 1 ) , where ta is the average experiment time and T1 the spin-lattice relaxation time. The enhancement factor of flow over static measurements for slowly relaxing carbon nuclei (T1 about 50–85 s) is between 3.5 and 5.0 and is between 1.5 and 2.5 for rapidly relaxing carbons (T1 about 5–10 s) in α-pinene. Choice of flow rate, pulse repetition time, evolution period, and spectral resolution, as well as the value of T1's, all affect experimental sensitivity enhancement for 2D flow NMR spectra." @default.
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- W2051236656 date "1987-07-01" @default.
- W2051236656 modified "2023-09-25" @default.
- W2051236656 title "Sensitivity enhancement for 13C-1H 2D J-resolved NMR using a recycled-flow method" @default.
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- W2051236656 doi "https://doi.org/10.1016/0022-2364(87)90009-6" @default.
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