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- W2051237649 abstract "2- and 4-Acetylpyridines, and 2- and 4-pyridinealdehydes when allowed to react with two-equiv. of aqueous titanium trichloride add to the carbonyl carbon atom of simple ketones (acetone, cyclopentanone, cyclohexanone) and aldehydes (acetaldehyde, propionaldehyde, benzaldehyde) affording subatituted pyridylglycols in very good yields. The present one-pot method has considerable advantage over the existing procedure. The reaction is discussed in terms of a radical mechanism in which the Ti(III) species plays the fundamental role." @default.
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- W2051237649 date "1983-01-01" @default.
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- W2051237649 title "A convenient synthesis of substituted pyridylgycols promoted by aqueous titanium trichloride" @default.
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- W2051237649 doi "https://doi.org/10.1016/s0040-4020(01)91888-5" @default.
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