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- W2051240548 abstract "Abstract Contact masses based on MgO and SiO 2 and mixtures thereof have been prepared, characterized (temperature-programmed desorption, UV spectroscopy, electron microscopy, energy-dispersive X-ray scanning transmission electron microscopy and X-ray diffraction) and tested in the direct synthesis of 1,3-butadiene from ethanol. The MgO/SiO 2 catalyst prepared by wet-kneading the components is distinguished from the mechanical mixture MgO+SiO 2 not only by its activity but also by its stability under steady-state conditions. This suggests that in the catalyst there is an interaction between the solids: a synergic effect. The physicochemical measurements confirm significant MgO-structural perturbations, particularly in the catalyst, occasioned by MgO-SiO 2 interactions. TPD results indicate an accumulation on the surface of oxygenated C 2 -species at the steady state, but apparently not oxygenated C 4 -entities." @default.
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- W2051240548 date "1988-01-01" @default.
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- W2051240548 title "Transformation of ethanol into 1,3-butadiene over magnesium oxide/silica catalysts" @default.
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- W2051240548 doi "https://doi.org/10.1016/s0166-9834(00)80905-7" @default.
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