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• W2051254182 abstract "We report a paired electrolysis method to prepare graphite nanoflakes (GNFs) and their supported noble metal/alloy nanoparticles (NM NPs/GNFs), by applying an alternating voltage (AV) on two graphite rod electrodes in a NaOH solution without/with noble–metal ions. The synthesis of GNFs might be related to the anodic exfoliation of graphite surface via OH− intercalation, accompanying the dispersion effect of hydrogen/oxygen gases evolution. The preparation of NM NPs/GNFs should be resulted from repeated coupling processes, namely the cathodic deposition of NM NPs and the electrochemical exfoliation-dispersion of NM NPs-decorated graphite layer. The as-prepared products were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy-disperse X-ray spectra (EDX), powder X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), atomic absorption spectroscopy (AAS) and inductively coupled plasma (ICP). The GNFs and NM NPs/GNFs exhibited high electrocatalytic activities toward the redox of 4-nitrophenol and oxidation of formic acid, respectively." @default.
• W2051254182 created "2016-06-24" @default.
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• W2051254182 date "2014-01-01" @default.
• W2051254182 modified "2023-10-18" @default.
• W2051254182 title "Preparation of Graphite Nanoflakes and Supported Noble Metal/Alloy Nanoparticles by Paired Electrolysis with Graphite Electrodes" @default.
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• W2051254182 doi "https://doi.org/10.1149/2.1211409jes" @default.
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