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- W2051255142 abstract "The one-electron oxidized linear pentanuclear nickel complexes [Ni(5)(tpda)(4)(H(2)O)(BF(4))](BF(4))(2) (1) and [Ni(5)(tpda)(4)(SO(3)CF(3))(2)](SO(3)CF(3)) (2) have been synthesized by reacting the neutral compound [Ni(5)(tpda)(4)Cl(2)] with the corresponding silver salts. These compounds have been characterized by various spectroscopic techniques. Compound 1 crystallizes in the monoclinic space group P2(1)/n with a = 15.3022(1) A, b = 31.0705(3) A, c = 15.8109(2) A, beta = 92.2425(4) degrees, V = 7511.49(13) A(3), Z = 4, and compound 2 crystallizes in the monoclinic space group C2/c with a = 42.1894(7) A, b = 17.0770(3) A, c = 21.2117(4) A, beta = 102.5688(8) degrees, V = 14916.1(5) A(3), Z = 8. X-ray structural studies reveal an unsymmetrical Ni(5) unit for both compounds 1 and 2. Compounds 1 and 2 show stronger Ni-Ni interactions as compared to those of the neutral compounds." @default.
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- W2051255142 date "2002-07-11" @default.
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- W2051255142 title "Unsymmetrical Linear Pentanuclear Nickel String Complexes: [Ni<sub>5</sub>(tpda)<sub>4</sub>(H<sub>2</sub>O)(BF<sub>4</sub>)](BF<sub>4</sub>)<sub>2</sub> and [Ni<sub>5</sub>(tpda)<sub>4</sub>(SO<sub>3</sub>CF<sub>3</sub>)<sub>2</sub>](SO<sub>3</sub>CF<sub>3</sub>)" @default.
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- W2051255142 doi "https://doi.org/10.1021/ic025582v" @default.
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