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- W2051260044 abstract "Abstract The fluorination of highly oriented pyrolytic graphite (HOPG), powdery and flaky natural graphites, and carbon fiber (P 100) has been performed in a fluorine atmosphere with HF gas (5.3 × 103−4.8 × 104 Pa), or by flowing fluorine gas in anhydrous liquid hydrogen fluoride (AHF) at ambient temperature. The obtained CxFs were the stage 1 to 2 compounds with composition of C1.9F to C7.0F. The stage 1 phases prepared from HOPG and pyrolytic graphite have shown large IC values of 1.12 nm to 1.18 nm. This result has coincided with the model that the stage 1 phase with large IC values is a bi-intercalation phase in which two kinds of almost ionically and semi-covalently bonded fluorine atoms with different C-F bond lengths are inserted in every other carbon layer. However, stage 1 CxF samples prepared from natural graphite powder and carbon fiber showed only one strong (001) diffraction line in most cases. X-ray powder diffraction and electron diffraction have revealed the absence of an in-plane superlattice at all stages." @default.
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- W2051260044 date "1994-01-01" @default.
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- W2051260044 title "Structure of fluorine-graphite intercalation compounds synthesized in gaseous and anhydrous liquid hydrogen fluoride with fluorine gas" @default.
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- W2051260044 doi "https://doi.org/10.1016/0008-6223(94)90216-x" @default.
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