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- W2051267254 abstract "The use of thin-film thermoplastic bonding to metals is an attractive option for future manufacturing. However the process has to be developed and the durability of these joints investigated. Grit blasting and Sodium Hydroxide Anodization (SHA) are used to modify titanium alloy (Ti-6A1-4V) specimens. The design of experiments used two voltages (10 and 15V) and times (15 and 30min) to create different surface morphologies. Titanium rods were then joined using poly ether ketone ether ketone ketone (PEKEKK) in thin-film form. The joined specimens were tensile tested before and after soaking in Ringer's solution (38°C) up to a period of six months. The surfaces were characterized using Profilometry, Scanning Electron Microscopy (SEM), and Energy Dispersive Spectroscopy (EDS). Joints created from anodization at 10 V for 30 min had very high initial tensile strengths of 134 MPa. Large diameter pores (∼100 nm) in the oxide were more attractive than smaller (∼30 nm) ones for PEKEKKTi adhesive joints under Ringer's solution soak. The adherends anodized at 15 V for 15 min retained 41% of their initial strengths after a soak period of six months, while the non-anodized joints retained only 6% of their initial strengths during the same period. The performance of anodized PEKEKK-Ti joints clearly exceeds non-anodized PEKEKK-Ti and other thermoset based joints for immersion soak periods to six months." @default.
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- W2051267254 date "1997-02-01" @default.
- W2051267254 modified "2023-10-13" @default.
- W2051267254 title "The effect of sodium hydroxide anodization on the durability of poly(etherketonetherketoneketone) adhesive bonding of titanium" @default.
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- W2051267254 doi "https://doi.org/10.1016/s0143-7496(96)00027-9" @default.
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