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- W2051279865 abstract "A mixture of Fe(II) and Fe(III) phenanthroline (phen) chelate complexes was isotachophoretically separated and analyzed by using a conventional electrolyte system for cation analysis (leading electrolyte: 20 mM ammonia solution, acetic acid buffer, pH 4.8; terminating electrolyte: β-alanine, pH 3.6). The migration order was Fe(III) chelate, Fe(II) chelate, phen. The recovery was 100% both for Fe(II) and Fe(III) according to PIXE analysis of the isotachophoretic (ITP) fractions. The sample mixture used (pH 2) was stable for a few days at room temperature. The sensitivity of Fe(III) chelate was 60% of that of Fe(II) chelate. This is because the ionic charge of Fe(II) chelate (+2) was larger than that of Fe(III) chelate, in which the coordination number of phen was 1.8±0.1 due to the addition of at least one pH buffer anion. The ionic charge of Fe(III) chelate was estimated as +1.4 by simulation of the concentration and effective mobility at the ITP steady state." @default.
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- W2051279865 date "1996-02-01" @default.
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- W2051279865 title "Isotachophoretic separation of Fe(II) and Fe(III) by using 1,10-phenanthroline as a complex-forming agent" @default.
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- W2051279865 doi "https://doi.org/10.1016/0021-9673(95)00884-5" @default.
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