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- W2051290230 abstract "A synthesis of the valuable amber-type odorant Ambrox® from labdanolic acid (main diterpenoid of the acid fraction of non-polar extracts of Cistus ladaniferus L.) is reported. The conversion is based on (a) the α,β-dehydrogenation of methyl labdanolate using an organoselenium reagent, (b) subsequent oxidative degradations of the side chain, and (c) final acid-promoted cyclization of the resulting tetranorlabdan-8α,12-diol. The influence of the temperature and solvent in the cyclization of the diol with p-toluenesulfonic acid is also described. Thus, Ambrox® has been obtained by a six-step procedure in 33% overall yield from methyl labdanolate." @default.
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- W2051290230 date "2002-07-01" @default.
- W2051290230 modified "2023-10-13" @default.
- W2051290230 title "Synthesis of Ambrox® from labdanolic acid" @default.
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- W2051290230 doi "https://doi.org/10.1016/s0040-4020(02)00571-9" @default.
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