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- W2051489077 abstract ": The profile of drying rate versus primary drying time for a spray freeze- dried trehalose aqueous solution is much different from that determined for regular freeze-drying. Drying rate declines very rapidly, attributed to rate-limiting heat transfer through the packed bed of frozen microparticles contained in a vial. The inter-particulate spaces appear to be the cause of this rate limitation. Use of either liquid nitrogen or liquid propane as a cryogenic produced strong differences in both SFD particle morphology and drying rate using trehalose, sucrose, or mannitol. The lack of any evident correlation supports the argument that the inter-particulate voids determine drying behavior. © 2009 Wiley-Liss, Inc. and the American Pharmacists Association J Pharm Sci 98:3447–3455, 2009" @default.
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- W2051489077 date "2009-09-01" @default.
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- W2051489077 title "Gravimetric Measurement of Momentary Drying Rate of Spray Freeze-Dried Powders in Vials" @default.
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- W2051489077 doi "https://doi.org/10.1002/jps.21677" @default.
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