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• W2052178295 endingPage "809" @default.
• W2052178295 startingPage "806" @default.
• W2052178295 abstract "Transition metal nitride halides MNX (M = Zr, Hf; X = Cl, Br, I) have two types of layer structured polymorphs, the alpha-form with the FeOCl type and the beta-form with the SmSI type. Both polymorphs consist of corrugated double M-N layers sandwiched between halogen layers, but with different atomic arrangements within the layers. The beta-form had been considered to be a high-temperature polymorph, because some beta-forms were obtained by thermal treatment of the corresponding alpha-forms. Here, the alpha-form was successfully transformed into the beta-form under high-pressure and high-temperature conditions; the new members of the beta-form were prepared for the first time from alpha-HfNBr, alpha-ZrNI, and alpha-HfNI using a high pressure of 3-5 GPa at 900 degrees C. The beta-form should be characterized as the high-pressure form rather than the corresponding high-temperature polymorph. This is the first high-pressure study on the polymorphs of metal nitride systems." @default.
• W2052178295 created "2016-06-24" @default.
• W2052178295 creator A5024509351 @default.
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• W2052178295 creator A5041129249 @default.
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• W2052178295 date "2000-02-01" @default.
• W2052178295 modified "2023-09-26" @default.
• W2052178295 title "High-Pressure Synthesis of the Polymorph of Layer Structured Compounds MNX (M = Zr, Hf; X = Cl, Br, I)" @default.
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• W2052178295 doi "https://doi.org/10.1021/ic991058l" @default.
• W2052178295 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/11272580" @default.
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