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• W2052231506 endingPage "5112" @default.
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• W2052231506 abstract "Abstract UV‐curable, transparent acrylic resin/titania organic–inorganic hybrid films were prepared by controlled hydrolysis of titanium tetrabutoxide in Span‐85/Tween 80 reverse micelles and the subsequent in situ photopolymerization of the acrylic monomers. UV–vis spectra and atomic force microscopy (AFM) indicated the presence of a nanoscale hybrid composition. The onset of absorption (λ onset ) of titania in the hybrids appeared between 363.4 and 383.5 nm, which exhibited blue shifts relative to that of bulk anatase (λ onset = 385 nm). The titania content increased rapidly at higher temperature and higher TTB content, whereas it increased slowly with longer post‐thermal treatment times. The refractive index and UV shielding properties of the organic polymer were obviously improved with increasing titania content. AFM images showed the inorganic domains (mean size 25.3–28.8 nm) were uniformly dispersed in the polymeric networks. The roughness parameters of the hybrid material were: toughness, 1.5–2.3 nm; root mean square roughness, 4.5–4.6 nm; and peak and valley distance, 9.7–19.4 nm. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 5105–5112, 2006" @default.
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• W2052231506 date "2006-09-28" @default.
• W2052231506 modified "2023-10-18" @default.
• W2052231506 title "Preparation of titanium dioxide/polyacrylate nanocomposites by sol–gel process in reverse micelles andin situ photopolymerization" @default.
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• W2052231506 doi "https://doi.org/10.1002/app.24166" @default.
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