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- W2052282170 abstract "When Pt(COD)Cl2 was treated with sodium amalgam in the presence of aromatic isocyanide (RNC, R = 2,6-Me2C6H3 (Xyl) or 2,4,6-Me3C6H2 (Mes)) and diphosphine with long methylene chain (diphos = Ph2P(CH2)nPPh2, n = 5 (dpppn) or 6 (dpphex)), two kinds of Hg-Pt mixed metal clusters, [Hg2Pt6-(diphos)2(RNC)8] (2) and [Hg2 Pt6(diphos)3(RNC)6] (3), were obtained. The structure of 3b (R Xyl, diphos dpphex) was determined by an X-ray analysis to be a cage-type cluster where a HG2 unit was incorporated into a trigonal-anti-prismatic platinum core, two Pt3 triangles being supported by three dpphex ligands (close-type). The cluster 2 was assumed to have an incomplete cage-type structure (open-type), and was converted to close-type 3 by treatment with an equivalent diphosphine ligand. When dppb (n = 4) was used, an open-type mixed metal cluster in which one mercury atom was captured, [HgPt6(dppb)2(RNC)8] (4), was obtained as the sole product." @default.
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- W2052282170 date "1992-11-01" @default.
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- W2052282170 title "Uptake of a Hg or Hg2 unit into the center of cage-type platinum clusters supported by diphosphines having long methylene carbon chains: X-ray structure of [Hg2Pt6(dpphex)3(RNC)6] · 2C6H6 (dpphex = 1,6- bis(diphenylphosphino)hexane, R = 2,6-dimethylphenyl)" @default.
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- W2052282170 doi "https://doi.org/10.1016/0022-328x(92)83478-z" @default.
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