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- W2052476093 abstract "A new cyano-bridged binuclear 4f-3d complex Sm(DMSO)4-(H2O)3Cr(CN)6 was synthesized and characterized by single crystal structure analysis. It crystallizes in monoclinic, space group P21 with a=0.9367(2) nm, b = 1.3917(3) nm, c = 1.1212(2) run, β = 99.88(3)° and Z = 2. In this binuclear complex, Sm atom is eight coordinated and linked to the Cr atom by a cyano bridge. The molecules packs to form 3D structure due to the hydrogen bonds among them. [K3(18-C-6)3(H2O)4]Cr(CN)6·3H2O (18-C-6 represents 18-crown-6-ether) that was synthesized as a byproduct in the preparation of a Gd—Cr complex is also structurally characterized. Crystal data: triclinic, space group P-l with a = 1.0496(7) nm, b= 1.1567(14) nm, c = 1.3530(13) nm, a = 94.15(9)°, β = 96.04(8)°, γ = 95.25(9)° and Z = l. [K3(18-C-6)3(H2O)4]-Cr(CN)6·3H2O consists of ionic [K3(18-C-6)3(H2O)4]3+ and [Cr(CN)6]3- pairs, of which the [K3(18-C-6)3(H2O)4]3+ ion is a trinuclear duster connected by water, and K atoms are eight coordinated by eight oxygen atoms of one 18-C-6 and two water molecules." @default.
- W2052476093 created "2016-06-24" @default.
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- W2052476093 date "2010-08-26" @default.
- W2052476093 modified "2023-09-25" @default.
- W2052476093 title "Assembly of a New Cyano-bridged 4f-3d Dimer Sm(DMSO)4- (H2O)3Cr(CN)6 and Crystal Structure of [K3(18-crown-6)3-(H2O)4]Cr(CN)6·3H2O" @default.
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- W2052476093 doi "https://doi.org/10.1002/cjoc.20030210326" @default.
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