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- W2052542107 abstract "Zwei unabhängige Verfahren (Fällung aus wäßriger Lösung und Festkörperreaktion) zur Darstellung vom vorher unbekannten Na5AlF2(PO4)2 wurden optimiert. Die Kristallstruktur wurde mit Diffraktometerdaten aufgeklärt (P3, a = b = 10,483(1), c = 6,607(1) Å, MoKα, 1080 unabhängige Reflexe, Rw = 0,025). PO4-Tetraeder und AlO4F2-„Oktaeder”︁ sind über gemeinsame Ecken zu einem zweidimensional ausgedehnten Heteropolyanion verknüpft. Natrium befindet sich in miteinander verbundenen Röhren des [AlF2(PO4)2]-Teils der Struktur. Die aufgrund der Strukturmerkmale zu erwartende Natriumionenleitfähigkeit wird experimentell bestätigt. Na5AlF2(PO4)2: Synthesis, Crystal Structure and Ionic Conductivity Two different procedures (precipitation from aqueous solution and solid state reaction) for the synthesis of hitherto unknown Na5AlF2(PO4)2 were optimized. The crystal structure was determined using diffractometer data (P3, a = b = 10.483(1), c = 6.607(1) Å, MoKα, 1080 independent reflections, Rw = 0.025). PO4-tetrahedra and AlO4F2-“octahedra” are connected via common vertices forming a twodimensionally extended heteropolyanion. Sodium is located in interconnected spacings of the [AlF2(PO4)2]-part of the structure. Ionic conductivity as expected because of these structural features was affirmed experimentally." @default.
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- W2052542107 date "1987-04-01" @default.
- W2052542107 modified "2023-09-27" @default.
- W2052542107 title "Na5AlF2(PO4)2: Darstellung, Kristallstruktur und Ionenleitf�higkeit" @default.
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- W2052542107 doi "https://doi.org/10.1002/zaac.19875470421" @default.
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