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• W2052729988 abstract "IR laser-induced gas-phase photolysis of Fe(CO)5–SiH4 mixtures occurs as SiH4-photosensitized decomposition of Fe(CO)5 is accelerated by products of this decomposition and it results in deposition of amorphous Si/Fe nanocomposite films. Analyses of the deposited and subsequently annealed solid films were made by FTIR, Raman and X-ray photoelectron spectroscopy, X-ray diffraction and electron microscopy. The deposited films are amorphous, contain crystalline nanostructures of iron silicide FeSi2 and undergo atmospheric oxidation in topmost layers to iron oxide and hydrogenated silicon oxide. Upon annealing they develop nanocrystalline structures of ferrisilicate, Fe1.6SiO4, carbon-encaged iron disilicide, FeSi2, and very rare hexagonal (high-pressure) Fe surviving at ambient conditions. The mechanism of formation of these nanostructures is discussed in terms of gas-phase and solid-phase reactions." @default.
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• W2052729988 date "2012-01-01" @default.
• W2052729988 modified "2023-10-17" @default.
• W2052729988 title "IR laser photodeposition of a-Fe/Si films developing nanograins of ferrisilicate, iron disilicide and rare hexagonal iron upon annealing" @default.
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• W2052729988 doi "https://doi.org/10.1039/c1dt11587a" @default.
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