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• W2052809622 abstract "A reaction between vanadocene and bis(pentafluorophenyl)acetylene in benzene solution has produced the title compound, (η5-C5H5)2V[η2-C2(C6F5)2], in 66% yield. The product has been characterized by infrared, mass spectral, and electron spin resonance data, as well as by a single crystal X-ray diffraction study. The compound crystallizes in the monoclinic space group C2/c with a = 11.961(6), b = 10.010(5), c = 16.670(8) Å, β = 98.42(5)°, and ρcalc = 1.81 g cm-3 for Z = 4. Least-squares refinement based on 984 observed reflections led to an R value of 0.039. The molecule resides on a crystallographic two-fold axis. The VC(η2) bond length is 2.077(5) Å, while the VC(η5) distances range from 2.268(6) to 2.291(5) Å and average 2.282(8) Å. Within the acetylenic ligand the CC length is 1.269(9) Å, and the CCC(C6F5) angle is 142.3(4)°." @default.
• W2052809622 created "2016-06-24" @default.
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• W2052809622 date "1980-09-01" @default.
• W2052809622 modified "2023-09-23" @default.
• W2052809622 title "The formation and molecular structure of bis(η5-cyclopentadienyl)bis(pentafluorophenyl)-vinylenevanadium: an acetylene derivative of vanadocene" @default.
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• W2052809622 doi "https://doi.org/10.1016/s0022-328x(00)93567-8" @default.
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