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- W2052832074 abstract "A new general synthesis of β-keto-enolates is described, whereby diketen is caused to react with various organic derivatives of aluminium, boron, and tin. Diketen thus reacts differently from its monomer (which affords C-acetyl derivatives). This is attributed to the unsymmetrical structure of the dimer. The symmetrical phenyl isocyanate dimer behaves similarly to its monomer in its reaction with trisdimethylaminoborane. The β-keto-enolates are characterised by elemental analyses, molecular weights, spectroscopic data (i.r., u.v., n.m.r., and mass spectrometry), and, in some cases, by chemical degradation or alternative methods of synthesis." @default.
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- W2052832074 date "1969-01-01" @default.
- W2052832074 modified "2023-09-23" @default.
- W2052832074 title "Chloroboration and allied reactions of unsaturated compounds. Part IX. Organometallic insertion reactions of diketen; synthesis of β-keto-enolates" @default.
- W2052832074 doi "https://doi.org/10.1039/j19690000173" @default.
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