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- W2052842127 abstract "Abstract Treatment of the carbon disulfide adducts FpCS 2 K and Fp′CS 2 K [Fp′=( η 5 -C 5 H 4 CH 3 )Fe(CO) 2 ] with Cp 2 ZrCl 2 affords the μ -( η 1 -C: η 2 -S,S′) dithiocarboxylate complexes FpCS 2 ZrClCp 2 ( 1 ) and Fp′CS 2 ZrClCp 2 ( 2 ). Both stable products were fully characterized. Metathesis between FpCS 2 K and Cp 2 ZrCl(OCMe 3 ) provided FpCS 2 Zr(OCMe 3 )Cp 2 ( 3 ), which was not obtained analytically pure. This product was characterized by comparison of its IR and 1 H-, 13 C{ 1 H}-NMR spectral data with that for 1 and 2 . The iron–zirconium complex FpZr(OCMe 3 )Cp 2 ( 4 ) was transformed by one equivalent of CS 2 to 3 (75% spectroscopic yield), a reaction that did not occur for FpZrClCp 2 . An insertion pathway is discussed for incorporating the CS 2 into the Fe–Zr bond of FpZr(OCMe 3 )Cp 2 ." @default.
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- W2052842127 date "1998-09-01" @default.
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- W2052842127 title "Characterization of the μ-(η1-C: η2-S,S′) dithiocarboxylate complexes Cp(CO)2Fe–CS2–Zr(X)Cp2 (X=Cl, OCMe3); CS2 insertion into the FeZr bond of the heterobimetallic complex Cp(CO)2Fe–Zr(OCMe3)Cp2" @default.
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- W2052842127 doi "https://doi.org/10.1016/s0022-328x(98)00752-9" @default.
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