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- W2052893998 abstract "In this study, we show a synthesis of λ-Ti3O5 nanocrystals dispersed in silica by sol–gel method. The X-ray diffraction measurements, Rietveld analyses, and transmission electron microscope images of the obtained samples showed that tuning the sintering temperature in the synthesis process can control the size of the λ-Ti3O5 nanocrystals, i.e., 8±2 nm (1123°C; sample 1), 9±3 nm (1133°C; 2), 9±2 nm (1143°C; 3), 10±3 nm (1153°C; 4), 11±4 nm (1163°C; 5), 13±4 nm (1173°C; 6), 25±12 nm (1200°C; 7), and 36±15 nm (1250°C; 8), whereas adjusting the hydrogen flow rate can tune the oxidation-reduction state of the sample without apparent change in the crystal size. At the lowest sintering temperature of 1123°C, the smallest X-Ti3O5 nanocrystals of 8 nm in size were produced." @default.
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- W2052893998 date "2014-03-06" @default.
- W2052893998 modified "2023-10-17" @default.
- W2052893998 title "Sol–gel synthesis of nanosized λ-Ti3O5 crystals" @default.
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- W2052893998 doi "https://doi.org/10.1088/1757-899x/54/1/012008" @default.
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