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• W2052917991 abstract "We present a WDS analytical technique for the determination by electron microprobe of low concentrations of the transition elements Sc, Ti, V, Cr, Mn, Co and Ni in ferro-magnesian silicate minerals. The quality of measurements is improved by: (1) Optimization of counting times, taking into account the anticipated analytical precision. (2) Monitoring instrumental and sample stabilities, by a statistical analysis of peak and background intensity values sampled at intervals of 1 s. Simultaneous measurement of major elements is essential in evaluating bias related to instrumental drift. (3) Precise determination of background, achieved by a least-squares fitting of the measured background to a calculated one. The latter is calculated by using a modified form of the Kramer's equation. This approach is also effective in correcting peak overlap interferences. The efficiency of this method was checked by performing core-to-rim analysis of garnet, clinopyroxene and orthopyroxene prophyroclasts in the peridotite nodule PHN 1611. This led to precise determination of trace-element chemical zoning in these minerals." @default.
• W2052917991 created "2016-06-24" @default.
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• W2052917991 date "1990-06-01" @default.
• W2052917991 modified "2023-09-29" @default.
• W2052917991 title "Electron microprobe determination of minor and trace transition elements in silicate minerals: A method and its application to mineral zoning in the peridotite nodule PHN 1611" @default.
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• W2052917991 doi "https://doi.org/10.1016/0009-2541(90)90140-3" @default.
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