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- W2052972727 abstract "Solid-phase organic synthesis (SPOS) was employed in the construction of isoxazole and/or isoxazoline polyheterocyclic systems. The [3 + 2] cycloaddition reactions of nitrile oxides, generated from the corresponding primary nitro compounds, with resin-bound alkynes or alkenes were highly efficient both chemically and with regard to purification. A parallel solution-phase synthesis was carried out which compared the synthetic efficiency in both media. SPOS of isoxazole/isoxazoline 11, employing a functionalized polystyrene resin, was found to be more efficient than the solution-phase approach. Three other oligoisoxazoles were prepared with average yields per step being 82, 84, and 89%." @default.
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- W2052972727 date "1997-10-01" @default.
- W2052972727 modified "2023-09-24" @default.
- W2052972727 title "Solid-Phase Synthesis of Isoxazoles and Isoxazolines: En Route to a New Class of Ionophores" @default.
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- W2052972727 doi "https://doi.org/10.1021/jo970712g" @default.
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